Reach Us +44 7480022449


Electro-Organic Synthesis Of 2-Amino-9(4-Chlorophenyl)-5,7,8,9- Tetra Hydro-6H Benzo [7] Annulen-6-One in Acidic Medium

The electro reduction of 5-(2-chlorophenyl)-1, 3- dihydro-7-2H-1, 4-benzodiazepin-2-one (clonazepam) has been studied by cyclic voltammetry at glassy carbon electrodes under the acidic conditions which indicate the reducible behavior of the drug. Electro-reduction of clonazepam has also been studied by the Galvanstatic technique at copper and amalgamated forms of copper and lead electrodes under acidic conditions. The reduction product was isolated and characterized by TLC, usual laboratory qualitative tests and IR, NMR spectral analysis. Effect of different parameters like current density, temperature, depolarizer concentration and nature of cathode material on yield percentage and current efficiency has been investigated. Number of electrons have also been calculated to confirm the isolated product, which is 2-amino-9- (4-chlorophenyl)-5,7,8,9-tetrahydro-6Hbenzo[ 7]annulen-6-one.


Abstract | Full-Text | PDF

Share this  Facebook  Twitter  LinkedIn  Google+
30+ Million Readerbase
Recommended Conferences
Flyer image
Abstracted/Indexed in
  • Chemical Abstracts Service (CAS)
  • Index Copernicus
  • Google Scholar
  • Genamics JournalSeek
  • China National Knowledge Infrastructure (CNKI)
  • CiteFactor
  • Scimago
  • Directory of Research Journal Indexing (DRJI)
  • WorldCat
  • Publons
  • MIAR
  • ResearchGate
  • University Grants Commission
  • Secret Search Engine Labs


tempobet giriş

tempobet giriş

tipobet süpertotobet yeni adres süperbahis 747 güvenilir bahis siteleri telefonda sex sohbet